Occasionally, I recognize a serious gap in my learning. For instance, what effect does eisbocking have on the gravity of a beer when I know that I’m not getting 100% water from skimming? What about the bourbon addition? What do the changes do to the overall hydrometer measurement of the beer? I suppose recognizing my gaps is good because it’s a chance to look into the process a bit more.
This eisbock portion was, by far, the most tedious point in the process of making this beer (you can find my earlier posts on this topic listed at the end of this article). Freezing a high viscosity beer, which is full of alcohol, in a conventional freezer is a serious pain. I was able to achieve—maybe—negative 7° Fahrenheit. By any stretch of the imagination, this is a very cold temp but perhaps not high enough. I’ve repeated again and again that my real issue was viscosity; I was able to freeze the beer, but due to the viscosity, I lost some entrenched beer in the process.
The eisbocking stage of my beer really helped me to understand why some of these big beers cost so much. Of course, my process was less efficient than a brewery’s might be, but I went from slightly more than eight twelve-ounce beers down to two twelve-ounce portions. I started with about 100 ounces of liquid and ended up with ounces. It really shows how the reduction of volume is massive in such a process.
As I mentioned in the last post, the gravity reading I got after the bourbon addition was 1.075, and I figured on 2.7319% actual alcohol increase (…etc.) for every 1% on the hydrometer. The effect of the ethanol remains proportional to the relative buoyancy of the solution (I may be off base on this because I’m admittedly more ignorant than I’d like to be about the topic. But the relative effect of density and water removal seemed to imply that my buoyancy effect would be consistent in this manner. I’m learning as I go). The way I approached this, hoping for absolute accuracy, was to use the difference in gravity of the initial beer to the finished eisbock solution to get my ABV change. Once I had done that, I need my multiplication of 2.7319 (noted above) times the hydrometer change, giving me my relative change. I wish that I could have bought a $50,000 piece of equipment that would simply give me my ABV. Or that I could have sent it to a lab. However, with 2 bottles and no cash, I did what I could.
Now for the million dollar question: what was the difference in the gravity?
The brew went from 1.075 to 1.095, which would mean 2.67107 on hydrometer*2.7319148 adjustment = 7.2971452+27.868857 = 35.166002% ABV. My ABV yield is still up in the air. Here’s the situation. I’ve reduced my volume by 3/4 (roughly), which (theoretically) means that I’ve reduced the water by 3/4 in the beer. This means that the ABV should be 3/4 of the original amount + original amount. So, 27.868*.75 = 20.901+27.8686 = 48.769% ABV.
Is this right? Who knows. The problem with the hydrometer becomes apparent at this point. Based on that calculation, the beer is roughly 35.166002%ABV. Which is it? I don’t know. Maybe at some point someone will read this article who really knows what they are talking about and can explain what’s going on. I’ve looked other places to try to find some answers, and it’s all over the map.
For instance, one person suggests reciprocation of the numbers. So, what they apparently mean is that if I reduced the volume to 1/4 of the original amount, then I can just multiply the original number by 4. So, according to that logic, my beer is now over 108% ABV…I seriously doubt that it’s purer than pure ethanol, but it does show how comical some of this stuff is. Truthfully, I think maybe the honest estimation is somewhere between the 35% & 48.7% results, and I may have even sunk the Bismark.
I’ve finally decided on a name for the beer: The Convoluted Truth. I think that has a nice ring to it.
There are some things I can know for certain. I accomplished what I set out to do originally: I beat the world’s strongest beer. I can’t help that the rules of the game changed in the meantime. I did beat Tactical Nuclear Penguin. So, I’m proud of that aspect of the process. I maybe even beat Sink the Bismark and the upcoming German beer that’s ostensibly 45% ABV. I’m afraid to make the latter claims. However, I’m not afraid to say that I had a lot of fun and learned a lot about brewing and myself. I’ve seen some gaps, improved my understanding, and found new avenues for exploration. I really wish I had a bottle to send everyone who reads this. If you meet me a Dark Lord Day, I’ll share a sip or two with you.
For some people, this whole thing is moot and pointless since I used this yeast, that yeast, or added bourbon. So be it, you don’t have to drink it. What I do know is that I used barley, yeast, hops, water and a bit of bourbon to make one of the biggest non-distilled (besides a bourbon addition) barley products that has ever existed. That’s enough for me, and I hope you enjoyed the posts (here they are in the original order: 1,2,3,4,5). I’m very proud of this accomplishment. Please tweet, re-tweet it, or re-re-tweet it or tell the L.A. Times to interview me about the site or something.
OK, this might seem like a simple solution, but have you considered taking a sample down to Lost Abbey and seeing if they will analyze your ABV? I’m assuming they have one of those $50,000 machines that can tell you your Alcohol content. I can’t believe that you only got 24 OZ of liquid left! I never would have guessed that, I assumed you would have at least a gallon or two. Great posts. And I really liked your idea of bringing a bottle to Idaho. After all if you only have two you should share with each side of the family…right? That would mean a bottle would be coming into the Gem state! WooHoo! Anyways, its been a great read either way.
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I meant that you would be a part of tasting it, too. Actually, I seriously doubt that the Lost Abbey has a machine like that. The Bruery and a lot of these more mid-size breweries don’t. Nate suggested to see if Berkley could test it or something. Maybe I’ll try to come up with a way to get it tested. It would have to be cheap or free because I’m not going to pay much to have a beer tested…unless I have a brewery.
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The real problem with volume is lack of Bourbon. I just didn’t want to keep spending money on Bourbon for such small amounts.
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Yeah…having read through your calculations it’s clear that there are so many variables that influence the final ABV, and you did a hell of a job. Most folks would have given up and said, “It’s a big beer.”
108% haha…
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beer_scientist Reply:
March 24th, 2010 at 8:04 am
Thanks, Nate. There was a ton to have to think about but I know that I achieved some of my goals.
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Mike, whether or not your calcs are right, this is a heck of an experiment! Kudos to you. You’ve learned some super valuable info that you can carry forward and you’ve been nice enough to share with the rest of us! Last night at the Beer vs WIne dinner, since I was sitting next to Garrett Oliver, I was able to talk to him about my Peanutbutter Porter. He gave me some great advice to improve it that he learned from his bacon beer. Just another example of how great beer folks are!
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beer_scientist Reply:
March 24th, 2010 at 8:01 am
That’s cool about Garrett Oliver. It’s just amazing what there is to learn and how much people are willing to help. I had a blast and am going to revisit this beer.
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Maybe I missed the most important part – what does it taste like?
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beer_scientist Reply:
March 24th, 2010 at 8:03 am
It’s actually very good Jim. It’s obviously boozy because of the strength. However, a ton residual sweetness and layers of chocolate, vanilla, roast and other flavors really props it up. I think it turned out great.
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[...] This post was mentioned on Twitter by Nate | THFB, Jeremy B and ThankHeavenForBeer, Michael Reinhardt. Michael Reinhardt said: https://tinyurl.com/yhzjo66 Homebrew making one of the strongest beers ever made! [...]
I’m pretty sure freezing beer to concentrate it is a form of distilling, but still a great experiment nonetheless!
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beer_scientist Reply:
March 24th, 2010 at 7:59 am
It was a great experiment. I’m eisbocking a Barley-wine now. I’m addicted.
Technically, distilling is the evaporation and recollection of alcohol. This is the removal of water. Distilling removes all but alcohol. Of course, this is why it’s legal to eisbock in a brewery but illegal to distill.
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[...] though they knew I was beating their strongest beers, Brew Dog still sent me the beer I ordered. I just wanted to show you a pic of what I got in the [...]
[...] One of the underlying assumptions is that this is an unseen and unheard phenomenon. Strong beer. I’m frightened, I’ve never heard of that before. (I’ve personally made a beer that’s stronger than TNP.) [...]
I dig the project, very cool.
However, as far as i’m concerned, Utopias still holds the record of world’s strongest beer.
It has the highest ABV ever reached by means of fermentation.
Eisbock methods are basically just a different way of saying “freeze-distilling”.
Just my opinion.
I still think this is a cool article, and i sincerely envy your in-depth brewing knowledge.
Also, i would definately love to try any/all of the brews made by “Brew Dog” and their dutch and german competitors during their little “who can freeze the most water out of their beer” contest.
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beer_scientist Reply:
December 21st, 2010 at 5:30 pm
Point taken. But I’m almost certain that Sam Adams also ages in spirit barrels. The highest fermenting yeast to date, that I know of, goes to 25% max (WLP 099). Granted that eisbocking is certainly a means to water removal. However, it is fundamentally different than distillation. Collection of nothing but alcohol being the the basic method of distillation. Removal of only water is a bit of a different beast because all else remain. I do get and understand your point though.
At the end of the day, it’s about drinking something good and pushing ourselves.
Thanks very much for the thoughtful and respectful response to my post. You are welcome to disagree any time you want and I hope to see you back here.
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aXxMgh Very true! Makes a canhge to see someone spell it out like that.
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